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Heptadecarodium Pentadecasulfide

Heptadecarodium pentadecasulfide is a binary inorganic compound of rhodium and sulfur with the formula Rh 17 S 15 , crystals.

Heptadecarodium Pentadecasulfide
General
Systematic
name
Heptadecarodium Pentadecasulfide
Traditional namesRhodium Sulphide
Chem. formulaRh 17 S 15
Physical properties
conditioncrystals
Molar mass2230.37 g / mol
Density7.6 g / cm³
Classification
Reg. CAS number52276-39-8

Getting

  • Sintering of stoichiometric amounts of pure substances or hydrothermal synthesis at 400 ° C [1] :
17Rh+fifteenS→TRh17Sfifteen{\ displaystyle {\ mathsf {17Rh + 15S \ {\ xrightarrow {T}} \ Rh_ {17} S_ {15}}}}  

Physical Properties

Heptadecarodium pentadecasulfide forms crystals of cubic syngony , space group P m 3 m , cell parameters a = 0.99103 nm, Z = 2, heptadecapalladium pentadecasulfide type structure Pd 17 S 15 [2] [3] [4] .

The compound goes into a superconducting state at a temperature of 2.2 K [5] .

Notes

  1. ↑ Wuxing Zhang, Kazumichi Yanagisawa, Sumio Kamiya, Tatsuo Shou. Phase Controllable Synthesis of Well-Crystallized Rhodium Sulfides by the Hydrothermal Method // Cryst. Growth Des .. - 2009. - T. 9 , No. 8 . - S. 3765–3770 . - DOI : 10.1021 / cg900454g .
  2. ↑ State Diagrams of Double Metal Systems / Ed. N.P. Lyakisheva. - M .: Engineering, 2000. - T. 3 Book 2. - 448 p. - ISBN 5-217-02932-3 .
  3. ↑ B. Predel. Rh-S (Rhodium-Sulfur) // Landolt-Börnstein - Group IV Physical Chemistry. - 1998. - T. 5 J. - S. 1-2 . - DOI : 10.1007 / 10551312_2610 .
  4. ↑ H. Okamoto. Rh-s (rhodium-sulfur) // Journal of Phase Equilibria. - 1992. - T. 13 , No. 1 . - S. 108-109 . - DOI : 10.1007 / BF02645398 .
  5. ↑ HR Naren, Arumugam Thamizhavel, AK Nigam, S. Ramakrishan. Superconductivity in Rh 17 S 15 and Pd 17 Se 15 : A Comparative Study // J. Phys. Soc. Jpn .. - 2011 .-- T. 80 . - S. SA014 . - DOI : 10.1143 / JPSJS.80SA.SA014 .


Source - https://ru.wikipedia.org/w/index.php?title= Pentadecasulfide heptadecarodium &oldid = 80368286


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