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Chloropentaamminrodium (III) Chloride

Chloropentaammaminrodium (III) chloride is an inorganic compound, a complex rhodium chloride with the formula [Rh (NH 3 ) 5 Cl] Cl 2 , yellow crystals, slightly soluble in water.

Chloropentaamminrodium Chloride
Are common
Systematic
name
Chloropentaamminrodium (III) Chloride
Traditional namesMonochloropentaminesminodichloride; rhodium purpureochloride
Chem. formula[Rh (NH 3 ) 5 Cl] Cl 2
Rat formula[RhCl (NH 3 ) 5 ] Cl 2
Physical properties
conditionyellow crystals
Molar mass294.42 g / mol
Density2.0 g / cm³
Chemical properties
Solubility in water0.836 g / 100 ml
Classification
Reg. CAS number13820-95-6
Reg. EINECS number

Content

Getting

  • Ammonium carbonate powder is added to a solution of rhodium (III) chloride and ammonium chloride (buffer):
2RhCl3+five(NHfour)2CO3→90oC2[Rh(NH3)fiveCl]Cl2↓+fiveCO2↑+fiveH2O{\ displaystyle {\ mathsf {2RhCl_ {3} +5 (NH_ {4}) _ {2} CO_ {3} \ {\ xrightarrow {90 ^ {o} C}} \ 2 [Rh (NH_ {3}) _ {5} Cl] Cl_ {2} \ downarrow + 5CO_ {2} \ uparrow + 5H_ {2} O}}}  
the precipitated crystals are washed with hot hydrochloric acid to wash out [Rh (NH 3 ) 4 Cl 2 ] Cl.

Physical Properties

Chloropentaammaminrodium (III) chloride forms yellow crystals of rhombic syngony , space group P nma , cell parameters a = 1.336 nm, b = 1.046 nm, c = 0.6741 nm, Z = 4 [1] .

Slightly soluble in water.

Chemical Properties

  • In aqueous solutions it reacts with cold concentrated nitric acid :
[Rh(NH3)fiveCl]Cl2+2HNO3+H2O→0oC[Rh(NH3)fourCl2]NO3⋅H2O↓+NHfourNO3+HCl{\ displaystyle {\ mathsf {[Rh (NH_ {3}) _ {5} Cl] Cl_ {2} + 2HNO_ {3} + H_ {2} O \ {\ xrightarrow {0 ^ {o} C}} \ [Rh (NH_ {3}) _ {4} Cl_ {2}] NO_ {3} \ cdot H_ {2} O \ downarrow + NH_ {4} NO_ {3} + HCl}}}  

Notes

  1. ↑ Robert S. Evans, Ernest A. Hopcus, Jon Bordner, Anton F. Schreiner. Molecular and crystal structures of halopentaamminerhodium- (III) complexes, [Rh (NH 3 ) 5 Cl] Cl 2 and [Rh (NH 3 ) 5 Br] Br 2 // Journal of Crystal and Molecular Structure. - 1973. - T. 3 , No. 4 . - S. 235-245 . - DOI : 10.1007 / BF01236644 .

Literature

  • Chemistry Handbook / Editorial: Nikolsky B.P. et al. - 3rd ed., rev. - L .: Chemistry, 1971. - T. 2. - 1168 p.
  • Inorganic Synthesis Guide: 6 Vol. / Ed. Brower, G. - Moscow : Mir, 1985 .-- V. 5 .-- 360 p.


Source - https://ru.wikipedia.org/w/index.php?title= Chloropentaamminrodium Chloride ( III)&oldid = 80372787


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