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Calcium thiocyanate

Calcium thiocyanate is an inorganic compound, a salt of calcium and rhodanic acid with the formula Ca (SCN) 2 , colorless (white) crystals, it dissolves in water, forms crystalline hydrates .

Calcium thiocyanate
Are common
Systematic
name
Calcium thiocyanate
Traditional namesCalcium thiocyanate; calcium thiocyanate
Chem. formulaCa (SCN) 2
Rac formulaCa (SCN) 2
Physical properties
conditioncolorless (white) crystals
Molar mass156.24 g / mol
Density2.1 g / cm³
Chemical properties
Water solubilitytetrahydrate - 59 g / 100 ml
Classification
Reg. CAS number65114-14-9
Reg. EINECS number218-244-3

Content

Getting

  • The effect of calcium oxide on ammonium thiocyanate :
CaO+2NHfourSCN→Ca(SCN)2+2NH3↑+H2O{\ displaystyle {\ mathsf {CaO + 2NH_ {4} SCN \ {\ xrightarrow {}} \ Ca (SCN) _ {2} + 2NH_ {3} \ uparrow + H_ {2} O}}}  

Physical Properties

Calcium thiocyanate forms colorless (white) crystals of monoclinic syngony , space group C 2 / c , cell parameters a = 0.9617 nm, b = 0.6424 nm, c = 0.7872 nm, β = 90.82 °, Z = four.

It is soluble in water and ethanol .

It forms crystalline hydrates of the composition Ca (SCN) 2 • n H 2 O, where n = 2, 3, and 4.

Crystalline hydrate Ca (SCN) 2 • 4H 2 O at 23.7 ° С [1] undergoes a phase transition in β-Ca (SCN) 2 • 4H 2 O, melts in its own crystallization water at 42.5–46.5 ° С , at 160 ° C is destroyed.

Crystalline hydrate Ca (SCN) 2 • 2H 2 O forms rhombic syngony crystals, space group P nma , cell parameters a = 1.2801 nm, b = 0.7903 nm, c = 0.7269 nm, Z = 4. [2]

Application

It is used as a mordant for dyeing or stuffing fabrics and as a solvent for cellulose , for mercerizing cotton, in medicine instead of potassium iodide (for treating atherosclerosis ), in the manufacture of parchment .

Notes

  1. ↑ Kirgintsev A.N., Trushnikova A.N., Lavrentieva V.G. Solubility of inorganic substances in water. - L .: Chemistry, 1972.- 248 p.
  2. ↑ Claudia Wickleder and Patrick Larsen. Ca (SCN) 2 and Ca (SCN) 2 • 2H 2 O: Crystal Structure, Thermal Behavior and Vibrational Spectroscopy // Z. Naturforsch .. - 2002. - V. 57 b . - S. 1419-1426 .

Literature

  • Chemist Handbook / Redkol .: Nikolsky B.P. et al. - 3rd ed., Rev. - L .: Chemistry, 1971. - T. 2. - 1168 p.
  • CRC Handbook of Chemistry and Physics . - 89th edition. - Taylor and Francis Group, LLC, 2008-2009.


Source - https://ru.wikipedia.org/w/index.php?title= Calcium thiocyanate&oldid = 100052297


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