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Calcium hexacyanoferrate (III)

Calcium hexacyanoferrate (III) is an inorganic compound, a complex salt of calcium and hexacyanoferric (III) acid with the formula Ca 3 [Fe (CN) 6 ] 2 , dissolves in water, forms crystalline hydrate - red crystals.

Hexacyanoferrate
Are common
Systematic
name
Calcium hexacyanoferrate (III)
Traditional namesCalcium iron synergy, calcium ferricyanide, calcium hexacyanoferriate
Chem. formulaCa 3 [Fe (CN) 6 ] 2
Physical properties
conditionhydrate - red crystals
Molar mass544.13 g / mol
Chemical properties
Solubility in waterdissolves

Content

Getting

  • Neutralization of hexacyanogen (III) acid with calcium carbonate :
3CaCO3+2H3[Fe(CN)6]→Ca3[Fe(CN)6]2+3CO2↑+3H2O{\ displaystyle {\ mathsf {3CaCO_ {3} + 2H_ {3} [Fe (CN) _ {6}] \ {\ xrightarrow {}} \ Ca_ {3} [Fe (CN) _ {6}] _ { 2} + 3CO_ {2} \ uparrow + 3H_ {2} O}}}  
  • Mixing a solution of calcium hexacyanoferrate (II) with a small excess of manganese hexacyanoferrate (III) and after filtering the precipitate, evaporate the resulting solution under vacuum [1] .


Physical Properties

Calcium hexacyanoferrate (III) forms a crystalline hydrate of the composition Ca 3 [Fe (CN) 6 ] 2 • 12H 2 O - red needle crystals, it dissolves well in water [2] [1]

Chemical Properties

The compound is stable in dry air when heated to 100 ° C and in a cold aqueous solution, however, when boiled in an aqueous solution it decomposes with the release of hydrocyanic acid , calcium hydroxide and precipitate of iron oxide (III) [1] :

Ca3[Fe(CN)6]2+9H2O→12HCN+Fe2O3↓+3Ca(OH)2{\ displaystyle {\ mathsf {Ca_ {3} [Fe (CN) _ {6}] _ {2} + 9H_ {2} O \ {\ xrightarrow {}} \ 12HCN + Fe_ {2} O_ {3} \ downarrow + 3Ca (OH) _ {2}}}}  


Application

  • A component of the epoxy polymerization catalyst [3] .

Notes

  1. ↑ 1 2 3 Williams HE The chemistry of cyanogen compounds and their manufacture and estimation . - London: J. & A. Churchill, 1915.
  2. ↑ Chemist's Handbook / Editorial: Nikolsky B.P. et al. - 3rd ed., rev. - L .: Chemistry, 1971. - T. 2. - 1168 p.
  3. ↑ Double metal cyanide complex catalysts modified with group iia compounds, 1999




Source - https://ru.wikipedia.org/w/index.php?title= Hexacyanoferrate ( III)_calcium&oldid = 80361991


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